TXRF Analysis

TX 2000 is the state of the art laboratory spectrometer for quantitative multi element trace analysis using Total Reflection X-Ray Fluorescence (TXRF).

TXRF is a type of Energy Dispersive X-Ray Fluorescence (EDXRF) in which the beam strikes the sample, deposited as a thin layer on a carrier, at a very small incidence angle, in order to exploit enhancement given by the total reflection effect. As far as the sample is thin enough (thin film approximation), the tecnique’s main strenghts are:

  •  simultaneous multi-element analysis from Na to Pu
  •  no matrix effect
  •  no matrix-dependent calibration curves
  •  improved detection limits (LOD) down to ng/g or lower
  •  minimum amount of sample
  •  microanalysis capabilities

 

TX 2000, equipped with an automatic primary beam switching system  (MoKa, WLa/Lb and bremsstrahlung 33 keV), a Silicon Drift Detector (SDD) and an high power X-Ray Tube is the optimal solution for applications in environmental, chemicals and nuclear fields.

 

TX 2000 Main Features

  • Stepper motors with optical encoders ensure extremely precise angular values.
  • Enhanced excitation mode by selection of the most suitable monochromatized energy (W-La/W-Lb/Mo-Ka) provided by the combination of double anode MO/W X-ray tube and W/Si multilayer. Other X-Ray anodes can be monochromatized as well.
  • Peltier-cooled Silicon Drift Detector with an energy resolution better than of 133eV (FWHM@MnKa, 1ms peaking time)
  • Minimal distance between the sample and the detector (mounted to the axis normal to the plane of the sample).
  • Instrumental detection limits below ng/g.
  • Helium flux attachment to improve the detection limits for the light elements.
  • No matrix effect
  • Environmental Analysis: water, dust, sediments, aerosol (ISO/TS 18507:2015, ISO 20289:2018)
  • Medical/Pharma: toxic elements in biological fluids and tissue samples, catalyst residues
  • Forensic Science: analysis of extremely small sample quantities
  • Pure chemicals: acids, bases, salts, solvents, water, ultrapure reagents
  • Oils and greases: crude oil, essential oil, fuel oil, gasoline, jet fuel
  • Pigments: ink, oil paints, powder
  • Nuclear Industry: measurements of radioactive elements

X-Ray Generator

  • Maximum Output Power: 3 kW
  • Max Output Voltage: 60 kV
  • Max Output Current: 60 mA
  • Voltage Step Width: 0.1 kV
  • Current Step Width: 0.1 mA

X-Ray Tube

  • TypeGlass, Mo/W anode, long fine focus
  • Focus 0.4 x 12 mm
  • Max Output 2.5 kW
  • Different anodes can be mounted on request

Multilayer monochromator

  • TypeW/Si
  • Reflectivity 80%

Excitation energies

  • W-La 8.4 keV (ΔE<1 keV)
  • W-Lb 9.67 keV (ΔE<1 keV)
  • Mo-Ka 17.44 keV (ΔE<1 keV)
  • Bremsstrahlung 33 keV

Sample Holder

  • 12 position sample holder

Detector

  • Active area: 40 mm2 as standard. (50 mm2 as option)
  • Energy resolution: ≤ 133 eV FWHM @Mn-Ka (1 μs peaking time)

Atmosphere

  • Air or He flux

Case

  • DimensionsWidth 580 mm, Height 1631.5 mm, Depth 793 mm
  • weight 200 kg (without chiller)
  • Leakage X-Rays< 1 mSv/Year (full safety shielding according to the international guidelines)

Cooling

  • External Chiller (1146h, 570w, 740d)

Software Informations

  • Least square Marquardt fit procedure for the area calculation (spectral analysis)
  • Automatic/manual search function
  • Manual or automatic calibration of energy
  • Quantification via an internal standard using theoretical and experimental sensitivity curves
 

Quality control

in metal analysis using OES/RDE

Material properties

control using XRD/TXRF

100%

Made in Italy

F.A.Q.

Even the most reliable equipment from ELVATECH may require service or repair. However, you need not worry as ELVATECH CANADA LTD. offers warranty and post-warranty service for spectrometers and analyzers at our company’s service center in Edmonton as well as at our authorized service center.

At Elvatech, our service concept is not centered around generating income but rather is a loyalty program for our customers. We offer fast, efficient, and non-profit maintenance and repair for our spectrometers. This approach significantly reduces the cost of using our spectrometers and analyzers and provides maximum convenience for our customers.

ELVATECH CANADA sells, rents, repairs, and provides service for XRF spectrometers and analyzers to customers all across Canada. Delivery is carried out by courier services directly from our head office in Edmonton based on CPT, Incoterms 2020.

Delivery time can vary from 1 to 12 weeks depending on the type of spectrometer, installed modes and calibrations, as well as availability of instruments in our stock.

Equipment is usually shipped after 100% payment is received to our bank account. Individual payment terms are provided for regular partners and dealers.

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